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Corona Discharge Micromachining for the Synthesis of Nanoparticles: Characterization and Applications [Kietas viršelis]

, (National Inst. of Tech. Karnataka, India)
  • Formatas: Hardback, 114 pages, aukštis x plotis: 216x138 mm, weight: 400 g, 22 Tables, black and white; 9 Line drawings, black and white; 5 Halftones, black and white; 14 Illustrations, black and white
  • Išleidimo metai: 25-Jun-2019
  • Leidėjas: CRC Press
  • ISBN-10: 0367224739
  • ISBN-13: 9780367224738
Kitos knygos pagal šią temą:
Corona Discharge Micromachining for the Synthesis of Nanoparticles: Characterization and ApplicationsDidesnis paveikslėlis
  • Formatas: Hardback, 114 pages, aukštis x plotis: 216x138 mm, weight: 400 g, 22 Tables, black and white; 9 Line drawings, black and white; 5 Halftones, black and white; 14 Illustrations, black and white
  • Išleidimo metai: 25-Jun-2019
  • Leidėjas: CRC Press
  • ISBN-10: 0367224739
  • ISBN-13: 9780367224738
Kitos knygos pagal šią temą:
Pastovi nuoroda: https://www.kriso.lt/db/9780367224738.html
Raktažodžiai:
This book summarizes the fundamental and established methods for the synthesis of nanoparticles, providing readers with an organized and comprehensive insight into the field of nanoparticle technology. In addition to exploring the characterization and applications of nanoparticles, it also focuses on the recently explored corona discharge micromachining - Electrical Discharge Micromachining (EDMM) - method to synthesize inorganic nanoparticles. In the synthesis of nanoparticles, organic materials often play an indispensable role, such as providing stabilizers in the form of capping agents.

This book will be of interest to advanced undergraduate and graduate students studying physics and engineering, as well as professionals and academics looking for an introduction to the nature and foundations of nanoparticle synthesis.

Features:











Provides diagnostic tools for the characterization of nanoparticles





Explores the cutting-edge EDMM method for the synthesis and characterization of nanoparticles





Discusses possible methods to overcome agglomeration of nanoparticles and achieve stable dispersion, in addition to examining the application suitability of synthesized nanoparticles
Preface xi
Notations xvii
Chapter 1 Introduction
1(1)
1.1 Fundamentals Of Nanoparticles
1(1)
1.2 Classification Of Nanoparticles
2(2)
1.3 Overview Of Application Of Nanoparticles
4(2)
1.4 Research On Nanoparticles
6(10)
1.4.1 Review on Nanoparticles Synthesis
6(4)
1.4.2 Review on Nanoparticles Stabilization and Application Characteristics
10(6)
1.5 Motivation
16(1)
1.6 Methodology
17(8)
References
18(7)
Chapter 2 Synthesis Methods
25(1)
2.1 Introduction
25(1)
2.2 Synthesis Methods
25(10)
2.2.1 Mechanical Methods
26(1)
2.2.1.1 Ball Milling Method
26(2)
2.2.1.2 Lithography Method
28(1)
2.2.2 Liquid Phase Reaction Methods
28(1)
2.2.2.1 Solution Precipitation Method
28(1)
2.2.2.2 Chemical Reduction Method
29(1)
2.2.2.3 Sol-Gel Method
29(1)
2.2.2.4 Electrochemical Method
29(1)
2.2.2.5 Micro-Emulsion Method
29(1)
2.2.2.6 Polyol Method
30(1)
2.2.2.7 BoilingFlask-3-Neck Method
30(1)
2.2.2.8 Microfluidic Reactor Method
30(1)
2.2.3 Vapor Phase Reaction Methods
31(1)
2.2.3.1 Wire Explosion Method
31(1)
2.2.3.2 Pulsed Laser Ablation Method
31(1)
2.2.3.3 Inert Gas Condensation Method
31(1)
2.2.3.4 Sputtering Method
32(1)
2.2.3.5 Chemical Vapor Condensation Method
32(1)
2.2.3.6 Submerged Arc Synthesis Method
32(1)
2.2.3.7 Combustion Flame Method
33(1)
2.2.3.8 Plasma Processing Method
33(1)
2.2.3.9 Aerosol Synthesis Method
33(1)
2.2.3.10 Spray Pyrolysis Method
34(1)
2.2.3.11 Solvated Metal Atom Dispersion Method
34(1)
2.2.3.12 Corona Discharge Micromachining--Electrical Discharge Micromachining (EDMM) Method
35(1)
2.3 Formulation Of Colloids
35(1)
2.4 Summary
36(3)
References
36(3)
Chapter 3 Diagnostic Methods
39(1)
3.1 Introduction
39(1)
3.2 Diagnostic Methods For Structural Characterization
40(5)
3.2.1 Scanning Electron Microscopy (SEM)
40(1)
3.2.2 Transmission Electron Microscopy (TEM)
41(1)
3.2.3 Energy Dispersive Analysis by X-Rays (EDAX)
41(1)
3.2.4 Selected Area Electron Diffraction (SAED)
42(1)
3.2.5 X-Ray Diffraction (XRD)
43(1)
3.2.6 Scanning Probe Microscopy (SPM)
44(1)
3.2.6.1 Scanning Tunneling Microscopy
44(1)
3.2.6.2 Atomic Force Microscopy
44(1)
3.3 Diagnostic Methods For Chemical Characterization
45(2)
3.3.1 UltraViolet-Visible (UV-Vis) Spectroscopy
45(2)
3.3.2 Ionic Spectrometry
47(1)
3.4 Diagnostic Methods For Application Characterization
47(8)
3.4.1 Ultrasonic Velocity Measurement
47(4)
3.4.2 Thermal and Electrical Conductivity Measurements
51(1)
3.4.3 Viscosity Measurement
52(3)
3.5 Summary
55(4)
References
56(3)
Chapter 4 A Novel Approach for Nanoparticles Synthesis--EDMM System
59(1)
4.1 Introduction
59(1)
4.2 Non-Conventional Machining Processes
60(4)
4.3 Electrical Discharge Machining (EDM)
64(4)
4.3.1 Salient Features of EDM
64(1)
4.3.2 EDM Cell
65(1)
4.3.3 Mechanism of EDM
66(2)
4.4 Electrical Discharge Micromachining (EDMM)
68(2)
4.4.1 EDMM Approach for Nanoparticles Synthesis
70(1)
4.5 Prototype Edmm System
70(5)
4.5.1 Ultrasonicator
72(1)
4.5.2 Piezoactuator
73(1)
4.5.3 Pulse Generation and Control Module
74(1)
4.5.4 Tool Feed Control Module
74(1)
4.6 Summary
75(4)
References
76(3)
Chapter 5 Synthesis, Characterization, and Application Suitability
79(1)
5.1 Introduction
79(1)
5.2 Synthesis Of Copper Nanoparticles
80(2)
5.2.1 Experimental Parameters
80(1)
5.2.2 Experimental Procedure
80(2)
5.3 Structural Characterization Of Synthesized Nanoparticles
82(11)
5.3.1 Colloidal Copper Nanoparticles
82(1)
5.3.1.1 Size, Shape, and Distribution in Pure DI Water
82(3)
5.3.1.2 Size, Shape, and Distribution in DI Water + PVA Solution
85(2)
5.3.1.3 Size, Shape, and Distribution in DI Water + PEG Solution
87(1)
5.3.2 Colloidal Aluminium Nanoparticles
88(1)
5.3.2.1 Size, Shape, and Distribution in Pure DI Water
88(3)
5.3.2.2 Size, Shape, and Distribution in DI Water + PEG Solution
91(1)
5.3.2.3 Size, Shape, and Distribution in DI water + BG Solution
92(1)
5.3.2.4 Size, Shape, and Distribution in DI Water + ACG Solution
92(1)
5.4 Chemical Characterization Of Synthesized Nanoparticles
93(5)
5.4.1 Optical Absorption of Colloidal Copper Nanoparticles
93(3)
5.4.2 Optical Absorption of Colloidal Aluminium Nanoparticles
96(2)
5.5 Application Characterization Of Synthesized Nanoparticles
98(10)
5.5.1 Concentration Measurement of Colloidal Nanoparticles
98(2)
5.5.2 Thermal Conductivity Measurement
100(1)
5.5.2.1 Colloidal Copper Nanoparticles
100(2)
5.5.2.2 Colloidal Aluminium Nanoparticles
102(1)
5.5.3 Viscosity Measurement
103(1)
5.5.3.1 Colloidal Copper Nanoparticles
103(3)
5.5.3.2 Colloidal Aluminium Nanoparticles
106(2)
5.6 Heat Transfer Application Of Colloidal Suspensions
108(3)
5.7 Summary And Conclusions
111(2)
5.8 Scope For Future Work
113(2)
References
113(2)
Index 115
Ranjeet Kumar Sahu received his BE degree in Mechanical Engineering in 2002 from Berhampur University, his M.Tech degree in Production Engineering in 2011 from NIT Rourkela, and his Ph.D in Nanomanufacturing from the Indian Institute of Technology Madras in 2016. Currently, he is working as a Research Assistant Professor in the Department of Mechanical Engineering at the SRM Institute of Science and Technology, Kattankulathur, India.



Somashekhar S. Hiremath works as an Associate Professor in the Department of Mechanical Engineering at the Indian Institute of Technology, Madras, Chennai, Tamil Nadu, India. He received his doctoral degree in 2004.