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Hybridizing Surface Probe Microscopies: Toward a Full Description of the Meso- and Nanoworlds [Kietas viršelis]

(University of Natural Resources and Life Sciences, Vienna, Austria), (University of Natural Resources and Life Sciences, Vienna, Austria)
  • Formatas: Hardback, 372 pages, aukštis x plotis: 234x156 mm, weight: 657 g, 15 Tables, black and white; 22 Illustrations, color; 166 Illustrations, black and white
  • Išleidimo metai: 08-Nov-2012
  • Leidėjas: CRC Press Inc
  • ISBN-10: 1439871000
  • ISBN-13: 9781439871003
Kitos knygos pagal šią temą:
Hybridizing Surface Probe Microscopies: Toward a Full Description of the Meso- and NanoworldsDidesnis paveikslėlis
  • Formatas: Hardback, 372 pages, aukštis x plotis: 234x156 mm, weight: 657 g, 15 Tables, black and white; 22 Illustrations, color; 166 Illustrations, black and white
  • Išleidimo metai: 08-Nov-2012
  • Leidėjas: CRC Press Inc
  • ISBN-10: 1439871000
  • ISBN-13: 9781439871003
Kitos knygos pagal šią temą:
Pastovi nuoroda: https://www.kriso.lt/db/9781439871003.html
Raktažodžiai:
"PREFACE Many are the books and reviews about scanning probe microscopies that cover the basics of their performance, novel developments and state-of-the-art applications. This book may appear to be another of this kind. But it is not. Indeed, this is not another book about scanning probe microscopy (SPM). As authors, we do not aim to focus on what SPM can do, but rather on what SPM cannot do and, most specifically, on presenting the experimental approaches that circumvent these limitations. The approaches are based on the combination of the SPM with two or more techniques that are complementary, in the sense that they can do something that the former cannot. This serves a double purpose: on the one hand, the so-resulting hybrid instrument outperforms the constituent techniques, since it combines their individual capabilities and cancels out their individual limitations. On the other hand, such instrument allows performing experiments of dissimilar nature in a simultaneous manner. But to understand the limitations of any technique also means to understand how this technique works. We do not skip this essential point; on the contrary, we have rather devoted a considerable amount of book space in explaining the basics of each technique as they are being introduced. In the case of SPM, we have endeavoured to present its fundamentals from a different, rather intuitive, perspective that, in our opinion, makes it distinctive from previous literature on the topic and it ultimately serves a pedagogical purpose. At the same time, we have tried to avoid explaining the particularities of each SPM-based technique and opted for a rather generalized approach that may suit everyone"--



Preface xi
Authors xiii
Chapter 1 Introduction
1(10)
Observing Nature: Sequentiality and Simultaneity
1(5)
Combination Macroscopic/Microscopic: Extending Measurable Range to Better Understand the Connection between Ultrastructure and Function
4(1)
Combination Model-Based/Direct Observation
4(1)
Making the Right Choice
4(1)
How to Judge the Applicability of a Model
5(1)
Combination Preparative/Measuring Technique
5(1)
Combination of Local Techniques to Track the Dynamics of Processes
6(1)
Combination of Local Techniques of Different Contrast
6(1)
Systems That Can Profit from Combined Techniques
6(2)
Living Cells
6(2)
Films
8(1)
Final Remarks
8(1)
References
9(2)
Chapter 2 Scanning Probe Microscopy as an Imaging Tool: The Blind Microscope
11(44)
Probe Imaging
11(40)
The SPM Family
24(1)
The Scanning Probe Microscope
25(1)
AFM
26(1)
STM
26(1)
Probes and Tips
26(2)
STM Probes
28(2)
AFM Probes
30(3)
Scanners
33(3)
Detection of the Tip's Position
36(1)
Tunneling Detection
36(1)
Optical Beam Detection
37(1)
Piezoresistive Detection
38(1)
SPM Imaging Modes
38(1)
Feedback Mechanism: Controlling the Property X
39(2)
Feedback in Contact Mode
41(1)
Feedback in Noncontact Mode
41(2)
Feedback in Intermittent-Contact Mode
43(1)
Topography and More: Feedback on X Mapping Y
44(2)
Artifacts in SPM Images
46(3)
Time Resolution in SPM Imaging
49(2)
Summary
51(2)
References
53(2)
Chapter 3 What Brings Optical Microscopy: The Eyes at the Microscale
55(64)
Fundamentals of Optical Microscopy
55(17)
Essential Parts of an Optical Microscope: The Image and Diffraction Planes
64(2)
Diffraction Sets the Limit of Detection, Spatial Resolution, and Depth of Focus
66(3)
Interference Sets Image Formation
69(1)
Optical Contrasts
69(1)
Phase Contrast
70(1)
Differential Interference Contrast
71(1)
Fluorescence Microscopy: Bestowing Specificity
72(9)
Optical Microscopy of Fluorescent Objects
77(1)
Light Source
78(1)
Collecting the Emitted Fluorescence: The Dichroic Mirror and the Emission Filter
78(2)
Drawbacks of Fluorescence Microscopy: The Ever-Present Photobleaching
80(1)
High-Performance Modes of Fluorescence Microscopy
81(14)
Confocal Laser Scanning Microscopy (CLSM)
81(2)
Fluorescence Lifetime Imaging Microscopy (FLIM)
83(3)
Total Internal Reflection Fluorescence (TIRF): A Near-Field Microscopy
86(1)
TIRF Is Based on the Optical Principles of Total Internal Reflection
86(1)
An Evanescent Wave Acts as the Excitation Source in TIRF
86(3)
Fluorescence Scanning Near-Field Optical Microscopy (Fluorescence SNOM)
89(4)
More than Near-Field Fluorescence Imaging
93(1)
Photobleaching or Background---Despite Weak and Highly Localized Illumination
93(2)
Optical Microscopies: Summary
95(1)
Combined OM-SPM Techniques: Eyesight to the Blind
95(11)
SPM and Optical Fluorescence Microscopy
98(8)
Fluorescence SNOM and Single-Molecule Detection
106(9)
Single Fluorescent Molecules as Test Samples
107(1)
Single-Molecule Imaging: Obtaining Molecular Orientations
108(1)
Conformations of Single-Polymer Chains in Films
109(2)
Single-Molecule Diffusion
111(1)
Distribution of Molecules and Molecular Complexes of Biological Interest in Synthetic and Native Membranes
112(3)
References
115(4)
Chapter 4 What Brings Scanning Near-Field Optical Microscopy: The Eyes at the Nanoscale
119(34)
Fundamentals of Scanning Near-Field Optical Microscopy
119(24)
Background Suppression
124(2)
The Nature of the SNOM Probe: Aperture and Apertureless SNOM
126(1)
Aperture SNOM
126(2)
Apertureless SNOM
128(3)
The History of SNOM Is the History of Its Probes
131(1)
Aperture Probes
132(3)
Apertureless Probes
135(1)
Tip-on-Aperture Probes
135(1)
Feedback Modes in SNOM
135(2)
Contrast Mechanisms in SNOM
137(3)
Polarization Contrast
140(2)
Refractive Index Contrast
142(1)
Infrared-Vibrational Contrast (Infrared Apertureless SNOM)
142(1)
Summary
142(1)
Applications of SNOM
143(6)
References
149(4)
Chapter 5 Adding Label-Free Chemical Spectroscopy: Who Is Who?
153(50)
Chemical Spectroscopy
153(13)
Raman (and IR) Microscopy
166(17)
Raman Microscopy beyond the Diffraction Limit: Near-Field Raman Spectroscopy
168(1)
Aperture Near-Field Raman Spectroscopy
169(1)
Tip-Enhanced Near-Field Raman Spectroscopy (TERS)
169(4)
Tip-Enhanced Coherent Anti-Stokes Raman Scattering (CARS)
173(1)
Sources of Enhancement of the Raman Signal in Near-Field Raman Spectroscopy
173(5)
IR Microscopy beyond the Diffraction Limit: IR Near-Field Spectroscopy
178(1)
Aperture SNOM + IR Spectroscopy
179(1)
Apertureless SNOM + IR Spectroscopy
180(2)
Another Source of Enhancement in Near-Field IR Microscopy: Phonon Excitation
182(1)
Summary
183(2)
Applications of SPM + Raman Spectroscopy
185(9)
(Sub-) Monolayers of Dyes
185(1)
Single-Wall Carbon Nanotubes
185(2)
Inorganic Materials: Silicon and Semiconductors
187(1)
Biomolecules
187(1)
Virus, Bacteria, and Human Cells
188(6)
Applications of SPM + IR Spectroscopy
194(5)
Inorganic Materials
194(1)
Polymers
194(1)
Viruses and Cells
195(4)
References
199(4)
Chapter 6 Combining the Nanoscopic with the Macroscopic: SPM and Surface-Sensitive Techniques
203(54)
Model-Based Surface Techniques
203(11)
Fundamentals of Surface Plasmon Resonance
214(7)
Surface Plasmons on Metal Surfaces
214(3)
Photon Creation/Excitation of SPPs
217(2)
Experimental SPR
219(2)
Fundamentals of Ellipsometry
221(8)
Basic Equation of Ellipsometry
221(1)
Single-Layer Model
222(3)
Experimental Determination of Ellipsometric Angles
225(1)
Rotating-Element Techniques
226(1)
Rotating Polarizer/Analyzer
226(1)
Rotating Compensator
227(1)
Phase Modulation
227(1)
Null Ellipsometry
228(1)
Fundamentals of Quartz Crystal Microbalance
229(12)
Electromechanical Analogy of a QCM Sensor: Equivalent Circuit of a Resonator
231(2)
Small-Load Approximation: Connecting Frequency Shifts to Load Impedance
233(2)
Measuring Frequency Shifts and More: Modes of Operation in QCM
235(1)
Impedance Analysis
235(1)
Ring-Down Technique
236(2)
Frequency Shifts and Viscoelastic Parameters: Some Case Examples
238(1)
The Special Case of Rigid Films in Air: Sauerbrey Equation and Film Thickness
238(1)
Viscoelastic Films and the Importance of Measuring at Different Overtones
239(2)
Main Drawback: The Importance of Qualitative Interpretation
241(1)
Summary
241(1)
The Combination SPM and Model-Based Surface Techniques
241(13)
SPM + SPR
241(3)
SPM + Ellipsometry
244(4)
SPM + QCM
248(6)
References
254(3)
Chapter 7 Scanning Probe Microscopy to Measure Surface Interactions: The Nano Push-Puller
257(46)
Force Curves: Surface Forces and More
257(11)
Measuring the Probe-Sample Interaction as a Function of the Relative Displacement
268(5)
Noise and Artifacts
272(1)
Quantitative Determination of Forces: Instrument and Cantilever Calibration
273(1)
Voltage to Deflection: Determination of the Sensitivity
273(7)
Deflection to Force: Determination of Spring Constant
273(4)
The Issue of Getting Absolute Distances
277(3)
Qualitative Interpretation of Force Curves
280(1)
Chemical Force Microscopy
281(1)
The Science of Pulling Single Molecules or Ligand-Receptor Pairs
282(8)
Statistical Description of Bond Rupture: Two-State Model
283(3)
Particularities of Molecular Recognition Spectroscopy
286(1)
Negative Controls
286(1)
Inferring Single Ligand-Receptor Interactions from Adhesion Events
287(1)
Particularities of Molecular Unfolding
288(2)
The Science of Pushing: Contact Nanomechanics
290(4)
A Short Note on Probes for Nanomechanics
290(1)
Contact Region of the Force Curve: Beyond the Point of Contact
291(3)
Mapping Interactions
294(4)
Force Curve Maps
294(2)
Pulsed Force Mode
296(1)
Molecular Recognition Imaging
297(1)
Summary
298(2)
References
300(3)
Chapter 8 Tidying Loose Ends for the Nano Push-Puller: Microinterferometry and the Film Balance
303(32)
Microinterferometry
303(4)
Fundamentals of Reflection Interference Contrast Microscopy
307(11)
Lateral and Vertical Resolution in RICM
311(1)
RICM Setup
312(2)
Dual-Wavelength RICM (DW-RICM)
314(1)
Applications of RICM
315(1)
RICM: Summary
316(2)
The Combined SPM/RICM Technique
318(3)
The Film Balance and Air-Fluid Interfaces
321(4)
Fundamentals of the Film Balance
325(4)
The Transfer of Monolayers onto Solid Supports
328(1)
The Langmuir-Blodgett Technique
328(1)
The Langmuir-Schaeffer Technique
328(1)
The Film Balance: Summary
329(1)
The Combined AFM + Film Balance: The Monolayer Particle Interaction Apparatus (MPIA)
329(4)
References
333(2)
Index 335
Susana Moreno Flores graduated with a degree in chemistry at the Complutense University (Madrid, Spain), where she also did her doctorate studies at the Department of Physical Chemistry. Thereafter she did postdoctoral stays at the Department of Statistical Physics of the Ecole Normale Supérieure (Paris, France), at the Max-Planck Institute of Polymer Research (Mainz, Germany) and at the Chemistry Department of the University of Basel (Basel, Switzerland), before she worked as researcher in the Biosurfaces Unit at CIC BiomaGUNE (San Sebastiįn, Spain). She is currently assistant professor at the Department of Nanobiotechnology of the University of Natural Resources and Life Sciences (Vienna, Austria).

José L. Toca-Herrera (Santander, Spain) is Professor of Biophysics at the University of Natural Resources and Life Sciences (BOKU-Vienna, Austria). After receiving his degree in Physics from the University of Valencia, he carried out a 12-month research training at the Max-Planck Institute for Polymer Research (Mainz) with Prof. Wolfgang Knoll. He completed his Ph.D. at the Max-Planck Institute of Colloids and Interfaces (Golm) under the supervision of Prof. Helmuth Möhwald. After several postdoctoral stays with Prof. Regine von Klitzing (TU-Berlin), Prof. Jane Clarke (University of Cambridge) and Prof. Uwe B. Sleytr (BOKU-Vienna), he joined in 2004 the Department of Chemical Engineering of the Rovira i Virgili University (Tarragona) as RyC research professor. In 2007 he moved to CIC BiomaGUNE (San Sebastiįn) led by Prof. Martin-Lomas as group leader. In September 2010, he joined the Department of Nanobiotechnology at BOKU (Vienna) where he leads the Laboratory of Biophysics.