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Laser-Induced Breakdown Spectroscopy 2nd edition [Minkštas viršelis]

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Edited by (Professor, Department of Physics, Banaras Hindu University, Varanasi, India), Edited by (Institute for Clean Energy Technology and Department of Physics and Astronomy, Mississippi State University Starkville, MS, USA)
  • Formatas: Paperback / softback, 620 pages, aukštis x plotis: 235x191 mm, weight: 1420 g
  • Išleidimo metai: 02-Jun-2020
  • Leidėjas: Elsevier Science Publishing Co Inc
  • ISBN-10: 0128188294
  • ISBN-13: 9780128188293
Kitos knygos pagal šią temą:
Laser-Induced Breakdown Spectroscopy 2nd editionDidesnis paveikslėlis
  • Formatas: Paperback / softback, 620 pages, aukštis x plotis: 235x191 mm, weight: 1420 g
  • Išleidimo metai: 02-Jun-2020
  • Leidėjas: Elsevier Science Publishing Co Inc
  • ISBN-10: 0128188294
  • ISBN-13: 9780128188293
Kitos knygos pagal šią temą:
Pastovi nuoroda: https://www.kriso.lt/db/9780128188293.html
Raktažodžiai:

Laser-Induced Breakdown Spectroscopy, Second Edition, covers the basic principles and latest developments in instrumentation and applications of Laser Induced Breakdown Spectroscopy (LIBS). Written by active experts in the field, it serves as a useful resource for analytical chemists and spectroscopists, as well as graduate students and researchers engaged in the fields of combustion, environmental science, and planetary and space exploration. This fully revised second edition includes several new chapters on new LIBS techniques as well as several new applications, including flame and off-gas measurement, pharmaceutical samples, defense applications, carbon sequestration and site monitoring, handheld instruments, and more.

LIBS has rapidly developed into a major analytical technology with the capability of detecting all chemical elements in a sample, of real- time response, and of close-contact or stand-off analysis of targets. It does not require any sample preparation, unlike conventional spectroscopic analytical techniques. Samples in the form of solids, liquids, gels, gases, plasmas, and biological materials (like teeth, leaves, or blood) can be studied with almost equal ease. This comprehensive reference introduces the topic to readers in a simple, direct, and accessible manner for easy comprehension and maximum utility.

  • Covers even more applications of LIBS beyond the first edition, including combustion, soil physics, environment, and life sciences
  • Includes new chapters on LIBS techniques that have emerged in the last several years, including Femtosecond LIBS and Molecular LIBS
  • Provides inspiration for future developments in this rapidly growing field in the concluding chapter
Dedication v
Contributors xi
Preface xv
I Basic physics and instrumentation
1 Fundamentals of LIBS and recent developments
Surya N. Thakur
Jagdish P. Singh
1 Introduction
3(1)
2 Lasers for LIBS
4(5)
3 Laser-induced plasmas
9(4)
4 Progress in detection of LIBS
13(4)
5 Applications of LIBS
17(2)
References
19(4)
2 Atomic emission spectroscopy
Surya N. Thakur
1 Introduction
23(1)
2 Atomic states and spectral lines
24(3)
3 Radiation from atoms
27(5)
4 Broadening of spectral lines
32(1)
5 Applications
33(6)
References
39(2)
3 Laser ablation
Richard E. Russo
X.L. Mao
J. Yoo
J.J. Gonzalez
1 Introduction
41(1)
2 Fundamental ablation processes
42(12)
3 Particle formation processes
54(1)
4 Laser ablation parameters
55(6)
5 Picosecond pulsed lasers
61(1)
6 Femtosecond pulsed lasers
62(4)
7 Perspectives, future, and trends
66(1)
Acknowledgment
66(1)
References
66(5)
4 Physics and dynamics of plasma in laser-induced breakdown spectroscopy
V.N. Rai
Surya N. Thakur
1 Introduction
71(1)
2 Basics of laser-matter interaction
72(1)
3 Processes in laser-produced plasma
73(1)
4 Spectral emission from plasma
74(1)
5 Models for the distribution of charged and excited states in plasma
75(2)
6 Measurement of spectroscopic and plasma parameters
77(4)
7 Characteristics of LIBS plasma
81(2)
8 Parameters affecting LIBS plasma
83(8)
9 Dynamics of plasma and its emission
91(2)
10 Effect of plasma parameters on LIBS emission
93(7)
11 Conclusion
100(1)
References
101(6)
5 Instrumentation for LIBS and recent advances
V.N. Rai
Surya N. Thakur
1 Introduction
107(1)
2 Typical LIBS setup
108(2)
3 LIBS instrumentation
110(4)
4 Fiber optic LIBS
114(3)
5 Portable LIBS devices
117(2)
6 Signal enhancement in LIBS
119(6)
7 Applications of LIBS
125(3)
8 Analytical performance of LIBS
128(1)
9 Conclusion
129(1)
References
130(9)
II New LIBS techniques
6 Ultrafast and filament-LIBS
S.S. Harilal
P.K. Diwakar
G. Miloshevsky
1 Introduction
139(2)
2 Nanosecond versus femtosecond LIBS
141(5)
3 Filamentation and filament-LIBS
146(3)
4 Emission and plume characteristics: Ultrafast LIBS versus filament-LIBS
149(2)
5 Modeling of ultrafast LIBS
151(10)
6 Summary
161(1)
Acknowledgment
161(1)
References
162(5)
7 Molecular laser-induced breakdown spectroscopy
Christian G. Parigger
David M. Surmick
Christopher M. Helstern
Ghaneshwar Gautam
Alexander A. Bol'shakov
Richard E. Russo
1 Introduction
167(2)
2 Experimental details of CN molecular emission spectroscopy
169(3)
3 Results and discussion of CN experiments
172(1)
4 Carbon Swan C2astrophysics emission spectra
173(3)
5 Plasma temperature distributions from AlO measurements
176(3)
6 Laser ablation molecular isotopic spectrometry
179(24)
7 Conclusions
203(1)
References
204(9)
III LIBS applications
8 Combustion applications of laser-induced breakdown spectroscopy
Fang Y. Yueh
Markandey M. Tripathi
Jagdish P. Singh
Banu Sezer
Kemal Efe Eseller
1 Introduction
213(1)
2 Continuous monitoring of combustion emission
214(2)
3 Equivalence ratio
216(3)
4 Online coal analysis
219(5)
5 Flame temperature
224(1)
6 Engine health
224(2)
7 Conclusions
226(1)
References
227(4)
9 LIBS application to liquid samples
Chet R. Bhatt
Christian L. Goueguel
Jinesh C. Jain
Dustin L. McIntyre
Jagdish P. Singh
1 Introduction
231(1)
2 Experimental details
232(1)
3 Optimization of experimental parameters
233(2)
4 LIBS signal enhancement techniques
235(1)
5 Underwater LIBS measurements
236(7)
6 Conclusions
243(1)
References
243(4)
10 LIBS application to powder samples
Chet R. Bhatt
Herve K. Sanghapi
Fang Y. Yueh
Jagdish P. Singh
1 Introduction
247(1)
2 Experimental
248(3)
3 Analytical methods
251(1)
4 Applications
252(7)
5 Conclusions
259(1)
References
260(3)
11 LIBS of slurry samples
K.K. Ayyalasomayajula
Fang Y. Yueh
Jagdish P. Singh
1 Introduction
263(1)
2 Experimental
264(3)
3 Results and discussion
267(6)
4 Conclusions
273(1)
Acknowledgments
273(1)
References
273(2)
12 Defense applications
Jennifer L. Gottfried
1 Introduction
275(2)
2 Identification of materials
277(18)
3 Material characterization
295(4)
4 Forensic analysis
299(4)
5 Future outlook
303(1)
Acknowledgments
304(1)
References
304(7)
13 Applications of LIBS in drug analysis
Pravin Kumar Tiwari
Pradeep Kumar Rai
Awadhesh Kumar Rai
1 Introduction
311(1)
2 Material and methods
312(5)
3 Results and discussion
317(10)
4 Conclusion and future outlook
327(1)
Acknowledgment
327(1)
References
328(1)
14 LIBS imaging applications
V. Motto-Ros
S. Moncayo
C. Fabre
B. Busser
1 Introduction
329(1)
2 Experimental
330(2)
3 Applications
332(10)
4 Summary and conclusion
342(1)
Acknowledgments
342(1)
References
342(5)
15 Food science application
Kemal Efe Eseller
Ismail Hakki Boyaci
Banu Sezer
Gonca Bilge
Halil Berberoglu
1 Introduction
347(1)
2 Experimental
348(4)
3 Food applications of LIBS
352(11)
4 Summary and conclusions
363(2)
References
365(4)
16 LIBS study of geological samples coupled with chemometric methods
Abhishek Kumar Rai
Jayanta Kumar Pati
Awadhesh Kumar Rai
1 Introduction
369(1)
2 LIBS experimental setup
370(1)
3 Analysis of geological samples
370(1)
4 Discrimination between rock types
371(1)
5 LIBS study of moldavite, a possible Martian analog
372(6)
6 Topsoil analysis using LIBS as a regolith proxy
378(4)
7 Conclusions
382(1)
References
382(2)
Further reading
384(1)
17 Study of the different parts of a tokamak using laser-induced breakdown spectroscopy
Gulab Singh Maurya
Pravin Kumar Tiwari
Rohit Kumar
Rajesh Kumar Singh
Awadhesh Kumar Rai
1 Introduction
385(1)
2 Experimental
386(1)
3 Results and analysis
387(11)
4 Conclusion
398(1)
Acknowledgments
398(1)
References
399(2)
18 High-energy materials application
Manoj Kumar Gundawar
1 Introduction
401(2)
2 Experimental details
403(1)
3 Spectral description
404(4)
4 Results and discussion
408(8)
5 Conclusion
416(1)
Acknowledgments
416(1)
References
416(5)
19 Industrial applications
Reinhard Noll
1 Introduction
421(4)
2 Inline measured 3D geometry information and LIBS analyses for high-speed sorting tasks of piece goods
425(3)
3 Sorting of refractories
428(1)
4 Sensor-based sorting of alloyed metal scrap
429(3)
5 Identification of steel blooms in a rolling mill
432(2)
6 Inverse production scenario for the recovery of valuable materials from electronic equipment
434(3)
7 Conclusion
437(1)
Acknowledgments
437(1)
References
437(4)
20 Laser-induced breakdown spectroscopy in planetary science
Roger C. Wiens
Xiong Wan
Jeremie Lasue
Sylvestre Maurice
1 Introduction
441(2)
2 ChemCam
443(12)
3 SuperCam LIBS
455(2)
4 MarsCode LIBS on the HX-1 Rover
457(4)
5 Indian lunar LIBS on Chandrayaan-2
461(5)
6 Future predictions
466(1)
Acknowledgments
467(1)
References
467(6)
21 Coal analysis
Zhe Wang
Zongyu Hou
Lei Zhang
Shunchun Yao
Sahar Sheta
Muhammad Sher Afgan
1 Introduction
473(1)
2 Main impact factors on coal analysis
474(4)
3 The application of LIBS to the offline analysis of coal
478(11)
4 The application of LIBS to the online analysis of coal
489(4)
5 Summary and future perspectives
493(1)
References
494(5)
22 LIBS for aerosol analysis
Daniel Diaz
David W. Hahn
Ulrich Panne
1 Introduction
499(2)
2 Laser-induced breakdown of gases
501(2)
3 Analysis of aerosol particles by LIBS
503(16)
4 Alternative methodologies for aerosol analysis
519(1)
5 Applications of LIBS-based aerosol analysis
520(4)
6 Future directions
524(3)
References
527(10)
23 Field-portable and handheld LIBS
Giorgio S. Senesi
Russell S. Harmon
Richard R. Hark
1 Introduction
537(1)
2 Instrumentation design, implementation, and attributes
537(4)
3 Portable, mobile, and handheld LIBS
541(3)
4 Applications of handheld LIBS
544(12)
5 Conclusions and perspectives
556(1)
References
556(4)
Further reading
560(1)
24 Self-calibrated methods for LIBS quantitative analysis
Stefano Legnaioli
Beatrice Campanella
Stefano Pagnotta
Francesco Poggialini
Vincenzo Palleschi
1 Introduction
561(2)
2 The calibration-free approach
563(2)
3 The CF-LIBS algorithm
565(4)
4 Other calibration-free approaches
569(3)
5 Applications
572(2)
6 Conclusion
574(1)
References
575(6)
25 Scope of future development in LIBS
Jagdish P. Singh
Fang Y. Yueh
Chet R. Bhatt
1 Introduction
581(1)
2 Gas-phase LIBS
582(1)
3 Liquid-phase LIBS
582(1)
4 Solid-phase LIBS
583(1)
5 LIBS of molten samples
583(1)
6 LIBS for biomedical applications
583(1)
7 A theoretical model of laser-induced plasma
584(1)
8 Commercialization of LIBS
585(1)
9 Future applications
585(3)
References
588(3)
Index 591
Dr. Singh received his M.Sc. and PhD from Banaras Hindu University, India. His field of specialization is Laser Spectroscopy, Optical Fiber Sensors, Explosive detection, Molecular Dynamics, Laser Diagnostics for Combustion, Laser Ultrasonic and Hazardous Waste Management. Dr. Singh is currently working on laser-based advanced optical diagnostics such as Laser Induced Breakdown Spectroscopy (LIBS) for measuring the composition of the Plutonium Oxide residue produced during weapons-grade Plutonium processing. He has developed LIBS for measuring the concentration of toxic metals in the off-gases and in melt glass. Dr. Singh has worked in laser photo fragmentation laser induced fluorescence (PF-LIF) to measure the concentration of explosives. Dr. Singh has also developed Non-linear laser diagnostic techniques such as Coherent Anti-Stokes Raman Spectroscopy for high temperature, high luminescence and turbulent combustion flows. He has published 165 papers in International Journals, 176 presentations and 8 patents. Dr. Singh is Fellow of OSA and LASSI. Surya N. Thakur is a retired Professor of Physics at Banaras Hindu University, India. He has taught courses in Physical Optics, Atomic Spectroscopy, Electronic & Vibrational Spectroscopy of Molecules, Spectro-Chemical Analysis, Lasers & Nonlinear Spectroscopy, Molecular Vibrations & Nonradiative Transitions and Experimental Techniques of Supersonic Molecular Beam Spectroscopy, Photoacoustic & Photothermal Spectroscopy, Optogalvanic Spectroscopy, and Raman Spectroscopy. He received his PhD in Experimental Spectroscopy from Banaras Hindu University and carried out postdoctoral work at Reading University, UK and SUNY Binghamton, USA. His interests are nonlinear spectroscopy, potential surfaces and nonradiative transitions in large molecules. He has held 1851 Exhibition Fellowship of the Royal Commission (London) and the Career Award of the University Grants Commission (New Delhi, India). He was President of the Physics Section of Indian National Science Congress in 1991 and is a Fellow of the Laser and Spectroscopy Society of India. He has over 100 research publications.