The effective investigation of corrosion requires the use of methods that can probe material surfaces at the atomic or molecular level and can be used in situ. This important collection reviews the range of techniques available and how they can be used to analyse different types of corrosion.
A number of chapters discuss the use of scanning probe microscopy techniques such as electrochemical scanning tunnelling microscopy and atomic force microscopy (EC-STM and EC-AFM). Other chapters analyse local electrochemical techniques such as scanning electrochemical microscopy (SECM), scanning vibrating electrode techniques (SVET), scanning droplet and scanning kelvin probe microscopy (SKFM), as well as microraman spectroscopy and photoelectrochemical imaging. The book reviews the application of these techniques in practice to various metals and types of coating as well as different kinds of corrosion.
With its distinguished editors and team of contributors, this is a valuable reference for all those concerned with corrosion research.
Local electrochemical methods in corrosion research; Observation of
self-healing functions on the cut edge of galvanised steel using SVET and pH
microscopy; Application of Scanning Vibrating Electrode (SVET) and Scanning
Droplet Cell (SDC) techniques to the study of weld corrosion; The use of SVET
to probe mechanistic changes in corrosion resistance of zinc aluminium
galvanising; Local analysis by SVET of the involvement of biological systems
in aerobic biocorrosion; Studying the delamination of organic coatings by
local electrochemical impedance spectroscopy; Initial stages of localised
corrosion by pitting of passivated nickel surfaces studied by Scanning
Tunnelling Microscopy (STM) and Atomic Force Microscopy (AFM); In situ Atomic
Force Microscopy (AFM) study of pitting corrosion and corrosion under strain
in a 304L stainless steel; Etching processes of ZnO (0001) surface in
solution studied by in situ Scanning Tunneling Microscopy; Scanning Kelvin
Probe Force Microscopy (SKPFM) applied to different conversion coated
aluminium surfaces; Using Scanning Kelvin Probe Force Microscopy (SKPFM) and
Scanning Kelvin Probe (SKP) to investigate the influence of microstructure on
the corrosion behaviour of magnesium alloys; The use of Scanning Kelvin Probe
Force Microscopy (SKPFM) and micro capillary cell techniques to investigate
local corrosion behaviour of 7xxx aluminium alloys; Atmospheric corrosion of
low alloy steels in a high humidity seashore environment; The influence of
surface microcracks on the pitting susceptibility of MnS-containing stainless
steels; Effect of applied stress on localised corrosion measurement of
aluminium alloy friction stir welding; In situ detection of galvanic coupling
during pitting using the Scanning Vibrating Electrode Technique (SVET) and
the Microcapillary Electrochemical Cell (MEC) method; Analysing thermal
oxidation using Micro Photo Electrochemistry (MPEC).
Dr Roland Oltra is Research Director at the Laboratoire de Recherches sur la Réactivité des Solides at the Université de Bourgogne, France. Dr Vincent Maurice works at the Laboratoire de Physico-Chimie des Surfaces at the Ecole Nationale Supérieure de Chimie de Paris (ENSCP-CNRS), France. Professor Robert Akid is Director of the Centre for Corrosion Technology at Sheffield Hallam University, UK Dr Philippe Marcus is Director of the Laboratoire de Physico-Chimie des Surfaces at ENSCP-CNRS, France. He is currently Vice-President of the European Federation of Corrosion (EFC) and Chair of EFC Working Party 6 (Surface Science and Mechanisms of Corrosion and Protection).