Understanding the Basics of Nanoindentation and Why It Is ImportantContact damage induced brittle fracture is a common problem in the field of brittle solids. In the case of both glass and ceramicsand as it relates to both natural and artificial bio-materialsit has triggered the need for improved fabrication technology and new product development in the industry.The Nanoindentation Technique Is Especially Dedicated to Brittle MaterialsNanoindentation of Brittle Solids highlights the science and technology of nanoindentation related to brittle materials, and considers the applicability of the nanoindentation technique. This book provides a thorough understanding of basic contact induced deformation mechanisms, damage initiation, and growth mechanisms. Starting from the basics of contact mechanics and nanoindentation, it considers contact mechanics, addresses contact issues in brittle solids, and explores the concepts of hardness and elastic modulus of a material. It examines a variety of brittle solids and deciphers the physics of deformation and fracture at scale lengths compatible with the microstructural unit block.Discusses nanoindentation data analysis methods and various nanoindentation techniquesIncludes nanoindentation results from the authors recent research on natural biomaterials like tooth, bone, and fish scale materialsConsiders the nanoindentation response if contact is made too quickly in glassExplores energy issues related to the nanoindentation of glassDescribes the nanoindentation response of a coarse grain aluminaExamines nanoindentation on microplasma sprayed hydroxyapatite coatingsNanoindentation of Brittle Solids provides a brief history of indentation, and explores the science and technology of nanoindentation related to brittle materials. It also offers an in-depth discussion of indentation size effect; the evolution of shear induced deformation during indentation and scratches, and includes a collection of related research works.
Section 1 Contact Mechanics. Contact Issues in Brittle Solids. Mechanics
of Elastic and Elastoplastic Contacts. Section 2 Journey Towards
Nanoindentation. Brief History of Indentation. Hardness and Elastic Modulus.
Nanoindentation: Why at All and Where?. Nanoindentation Data Analysis
Methods. Nanoindentation Techniques. Instrumental Details. Materials and
Measurement Issues. Section 3 Static Contact Behavior of Glass. What If the
Contact is Too Quick in Glass?. Enhancement in Nanohardness of Glass:
Possible?. Energy Issues in Nanoindentation. Section 4 Dynamic Contact
Behavior of Glass. Dynamic Contact Damage in Glass. Does the Speed of Dynamic
Contact Matter?. Nanoindentation Inside the Scratch: What Happens?. Section 5
Static Contact Behavior of Ceramics. Nanomechanical Properties of Ceramics.
Does the Contact Rate Matter for Ceramics?. Nanoscale Contact in Ceramics.
Section 6 Static Behavior of Shock-Deformed Ceramics. Shock Deformation of
Ceramics. Nanohardness of Alumina. Interaction of Defects with Nanoindents in
Shocked Ceramics. Effect of Shock Pressure on ISE: A Comparative Study.
Section 7 Nanoindentation Behavior of Ceramic-Based Composites.
Nano/Micromechanical Properties of C/C and C/C-SiC Composites.
Nanoindentation on Multilayered Ceramic Matrix Composites. Nanoindentation of
Hydroxyapatite-Based Biocomposites. Section 8 Nanoindentation Behavior of
Functional Ceramics. Nanoindentation of Silicon. Nanomechanical Behavior of
ZTA. Nanoindentation Behavior of Actuator Ceramics. Nanoindentation of
Magnetoelectric Multiferroic Material. Nanoindentation Behavior of
Anode-Supported Solid Oxide Fuel Cell. Nanoindentation Behavior of
High-Temperature GlassCeramic Sealants for Anode-Supported Solid Oxide Fuel
Cell. Section 9 Static Contact Behavior of Ceramic Coatings. Nanoindentation
on HAp Coating. Weibull Modulus of Ceramic Coating. Anisotropy in
Nanohardness of Ceramic Coating. Fracture Toughness of Ceramic Coating
Measured by Nanoindentation. Effect of SBF Environment on Nanomechanical and
Tribological Properties of Bioceramic Coating. Nanomechanical Behavior of
Ceramic Coatings Developed by Micro Arc Oxidation. Section 10 Static Contact
Behavior of Ceramic Thin Films. Nanoindentation Behavior of Soft Ceramic Thin
Films: Mg(OH)2. Nanoindentation Study on Hard Ceramic Thin Films: TiN.
Nanoindentation Study on Sputtered Alumina Films for Spacecraft Application.
Nanomechanical Behavior of Metal-Doped DLC Thin Films. Section 11
Nanoindentation Behavior on Ceramic-Based Natural Hybrid Nanocomposites.
Orientational Effect in Nanohardness of Tooth Enamel. Slow or Fast Contact:
Does it Matter for Enamel?. Anisotropy of Modulus in Cortical Bone.
Nanoindentation of Fish Scale. Section 12 Some Unresolved Issues in
Nanoindentation. Indentation Size Effect (ISE) and Reverse Indentation Size
Effect (RISE) in Nanoindentation. Pop-in Issues in Nanoindentation. Effect of
Loading Rate on Nanoindentation Response of Brittle Solids. Measurement of
Residual Stress by Nanoindentation Technique. Reliability Issues in
Nanoindentation Measurements. Substrate Effect in ThinFilm Measurements.
Future Scope of Novel Nanoindentation Technique. Conclusions. Common
Abbreviations. Index.
Dr. Arjun Dey is a scientist at the Thermal System Group of ISRO Satellite Centre, Bangalore. Dr. Dey earned a bachelors in mechanical engineering in 2003, followed by a masters in materials engineering from Bengal Engineering and Science University, Shibpur, Howrah in 2007. While working at CSIR-Central Glass and Ceramic Research Institute (CSIR-CGCRI), Kolkata, he earned his doctoral degree in materials science and engineering in 2011 from the Bengal Engineering and Science University, Shibpur, Howrah. The research work of Dr. Dey culminated in more than 120 publications to his credit.
Dr. Anoop Kumar Mukhopadhyay
is a chief scientist and head of the Mechanical Property Evaluation Section in the Materials Characterization Division of CSIR-CGCRI, Kolkata, India. He also heads the Program Management Division and Business Development Group of CSIR-CGCRI. He obtained his bachelors degree with honours in physics from Kalyani University, Kalyani in 1978 followed by a masters degree in physics from Jadavpur University, Kolkata in 1982. Dr. Mukhopadhyay has written nearly 200 publications including SCI journals, national and international conference proceedings. He has written seven patents and published three book chapters.
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